Metrohm, 6.100.6520, Metrosep A Supp 5 - 150/4.0
Catalog Number: 6.100.6520
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Category
| ApplicationRange | Applications Standard anions F - , Cl - , Br - , I - ClO 2 - , ClO 3 - , ClO 4 - , BrO 3 - Cr(VI) (CrO 4 2- ) Method development Difficult matrices Difficult separation problems |
|---|---|
| Organic Modifier | 0 - 100% (particularly acetone, acetonitrile, methanol) |
| Regeneration | Contamination with low-valency hydrophilic ions: a) Rinse with ultrapure water (25 min at 0.3 mL/min) b) Rinse with 10x concentrated eluent (100 min at 0.3 mL/min) c) Rinse with ultrapure water (25 min at 0.3 mL/min) d) Rinse with eluent (100 min at 0.3 mL/min) Contaminations with high-valency hydrophobic ions and organic contaminations: a) Rinse with ultrapure water (25 min at 0.3 mL/min) b) Rinse with 5% acetonitrile (20 min at 0.3 mL/min) c) Rinse with 100% acetonitrile (60 min at 0.3 mL/min) d) Rinse with 50% acetonitrile (10 min at 0.3 mL/min) e) Rinse with ultrapure water (50 min at 0.3 mL/min) f) Rinse with eluent (100 min at 0.3 mL/min) With shifted system peak (regeneration method with column oven): a) Rinse with concentrated eluent 1 mol/L Na 2 CO 3 (25 min at 0.4 mL/min) b) Maintain at 45 - 50 °C for 10 - 12 hours (without rinsing) c) Rinse with standard eluent (at least 40 min at 0.4 mL/min) |
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| StandardEluent |
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| Carbonate eluent (standard eluent) Sodium hydrogen carbonate: 1.0 mmol/L; 168 mg/2 L Sodium carbonate: 3.2 mmol/L; 678 mg/2 L Chromate eluent Sodium hydrogen carbonate: 4.0 mmol/L; 672 mg/2 L Sodium carbonate: 12.8 mmol/L; 2712 mg/2 L |
| Storage | In the eluent |
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| Capacity | 52 µmol (Cl – ) |
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| Housing material | PEEK |
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| Carrier material | Polyvinyl alcohol with quarternary ammonium groups |
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| Particle size | 5 µm |
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| Standard flow | 0.7 mL/min |
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| Maximum pressure | 15 MPa |
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| Maximum flow | 0.8 mL/min |
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| pH range | 3–12 |
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| Column dimensions | 150 x 4.0 mm |
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| Temperature range | 20–60 °C |
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